Use of switchable solvent liquid phase microextraction for determination of petroleum pollutants in water samples by gas chromatography–mass spectrometry

استفاده از میکرواستخراج فاز مایع با حلال قابل تغییر برای تعیین آلاینده‌های نفتی در نمونه‌های آب به روش کروماتوگرافی گازی-طیف‌سنجی جرمی

Author: Kobra Sadat Hasheminasab, Mahmood payehghadr, laleh dehghan nasab dolatabadi · 2023

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In this study switchable solvent liquid phase microextraction (SSLPME) followed by GC-MS detection has been developed for preconcentration and determination of total petroleum hydrocarbons (TPHs) in water samples. The extraction technique makes use of 100 μL of a water-immiscible solvent (dipropylamine) that can be solubilized in the aqueous phase in 1:1 ratio using HCl as a reagent. Afterwards, phases separation is induced by the addition of sodium hydroxide. Optimization of the variables af...

Details

Author
Kobra Sadat Hasheminasab, Mahmood payehghadr, laleh dehghan nasab dolatabadi
Year
2023
Class
Science & Knowledge
Type
Book
Source
DOAJ

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